Staff Publications

Staff Publications

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    'Staff publications' is the digital repository of Wageningen University & Research

    'Staff publications' contains references to publications authored by Wageningen University staff from 1976 onward.

    Publications authored by the staff of the Research Institutes are available from 1995 onwards.

    Full text documents are added when available. The database is updated daily and currently holds about 240,000 items, of which 72,000 in open access.

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Record number 371590
Title Systematic investigation of lard polymorphism using combined DSC and time-resolved synchrotron X-ray diffraction
Author(s) Kalnin, D.J.E.; Lesieur, P.; Artzner, F.; Keller, G.; Ollivon, M.
Source European Journal of Lipid Science and Technology 107 (2005)9. - ISSN 1438-7697 - p. 594 - 606.
DOI https://doi.org/10.1002/ejlt.200501010
Department(s) Physics and Physical Chemistry of Foods
Publication type Refereed Article in a scientific journal
Publication year 2005
Keyword(s) thermal-behavior - cocoa butter - fats - triglycerides - interesterification - crystallization - glyceride - phase
Abstract The polymorphic behavior of lard was systematically investigated by differential scanning calorimetry (DSC) while simultaneously monitoring the formation of the different crystal forms with X-ray diffraction (XRDT). To interpret the complex polymorphic evolution of the sample analyzed by regular DSC, both XRD patterns and DSC curves were recorded at the same time from the same sample (20 mg) using a laboratory-made calorimeter (http://www.umr-cnrs8612.u-psud.fr/Francais/pdf/MICROCALIX.pdf) installed at a synchrotron radiation bench capable of both small- and wide-angle X-ray diffraction and time-resolved experiments. Lard exhibits a large melting range (-30 degrees C
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