Staff Publications

Staff Publications

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    'Staff publications' is the digital repository of Wageningen University & Research

    'Staff publications' contains references to publications authored by Wageningen University staff from 1976 onward.

    Publications authored by the staff of the Research Institutes are available from 1995 onwards.

    Full text documents are added when available. The database is updated daily and currently holds about 240,000 items, of which 72,000 in open access.

    We have a manual that explains all the features 

Record number 320388
Title Screening for gestagens in kidney fat using accelerated solvent extraction and liquid chromatography electrospray tandem mass spectrometry
Author(s) Hooijerink, H.; Bennekom, E.O. van; Nielen, M.W.F.
Source Analytica Chimica Acta 483 (2003)1-2. - ISSN 0003-2670 - p. 51 - 59.
Department(s) BU Microbiological & Chemical Food Analysis
Publication type Refereed Article in a scientific journal
Publication year 2003
Keyword(s) supercritical-fluid extraction - tissues - steroids
Abstract A screening method has been developed for the determination of various anabolic steroids in kidney fat. Fat samples are extracted and steroids are trapped "on-line" during accelerated solvent extraction (ASE). Following this initial extraction samples are further purified with C18 solid-phase extraction (SPE). Compounds were finally analyzed by liquid chromatography (LC) coupled with tandem mass spectrometry (MS). The method was validated using blank kidney fat and fat samples fortified at 2 ng g-1. The detection capability (CC) was
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